骨松汤含药血清对H2O2诱导成骨细胞铁死亡的影响及机制
Effects and mechanism of Gusong Decoction-Containing serum on H2O2-induced ferroptosisin osteoblasts
  
DOI:10.3969/j.issn.1006-7108.2025.10.001
中文关键词:  骨松汤含药血清  过氧化氢  MC3T3-E1细胞  铁死亡  NOX4  成骨细胞
英文关键词:Gusong Decoction-containing serum  H2O2  MC3T3-E1 cells  ferroptosis  NOX4  osteoblasts
基金项目:国家自然科学基金面上项目(82374490);河南省卫生健康委国家中医临床研究基地科研专项(2021JDZX2121)
作者单位
王莉莎1 郭中华1* 王上增1 史栋梁1 张仲博1 任博文1 王云飞1 周晓宁2 王俊杰1 杨少祥1 1.河南省中医院骨病一科,河南 郑州 400002 2.河南省骨科医院颈肩腰腿痛四科,河南 郑州 450000 
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中文摘要:
      目的 探究骨松汤含药血清对过氧化氢(H2O2)诱导小鼠胚胎成骨细胞前体细胞(MC3T3-E1)铁死亡的影响及其作用机制。方法 采用细胞计数试剂盒(CCK-8)筛选骨松汤含药血清和铁抑制素-1(Fer-1)处理浓度。选择合适剂量的骨松汤含药血清和Fer-1干预,荧光探针检测亚铁离子(Fe2+)和活性氧(ROS)水平;酶联免疫吸附试验(ELISA)检测超氧化物歧化酶(SOD)、过氧化氢酶(CAT)、丙二醛(MDA)水平及碱性磷酸酶(ALP)活性;比色法检测谷胱甘肽(GSH)水平;茜素红S染色检测钙结节吸光度(OD)值;免疫印迹检测谷胱甘肽过氧化物酶4(GPX4)、长链脂酰-CoA合成酶4(ACSL4)和烟酰胺腺嘌呤二核苷酸磷酸氧化酶4(NOX4)蛋白表达。细胞过表达NOX4,检测铁死亡相关指标(GPX4和ACSL4蛋白表达、GSH水平、MDA含量)和细胞成骨功能(ALP活性和钙结节OD值)。结果 H2O2诱导MC3T3-E1细胞铁死亡。与H2O2组相比,骨松汤含药血清和Fer-1干预显著提高了细胞存活率、SOD和CAT活性、GSH水平以及GPX4蛋白表达(P<0.05),降低细胞MDA含量、Fe2+和ROS水平以及NOX4与ACSL4蛋白表达(P<0.05)。NOX4过表达抑制了骨松汤含药血清对H2O2处理MC3T3-E1细胞铁死亡和成骨功能的保护作用。结论 骨松汤含药血清能够抑制H2O2诱导的MC3T3-E1细胞铁死亡,这可能与其抑制NOX4/ROS信号通路活化有关。
英文摘要:
      Objective To investigate the effect of Gusong Decoction-containing serum on hydrogen peroxide (H2O2)-induced ferroptosis in mouse embryonic osteoblast precursor cells (MC3T3-E1) and its underlying mechanism. Methods The cell counting kit (CCK-8) was utilized to determine the optimal concentrations of Gusong Decoction-containing serum and Ferrostatin-1 (Fer-1) treatment. Subsequently, appropriate doses of Gusong Decoction-containing serum and Fer-1 were selected. Levels of ferrous ion (Fe2+) and reactive oxygen species (ROS) were measured using fluorescent probes. Superoxide dismutase (SOD), catalase (CAT), malondialdehyde (MDA) levels, and alkaline phosphatase (ALP) activity were assessed via enzyme-linked immunosorbent assay (ELISA). Glutathione (GSH) levels were determined using a colorimetric assay. The absorbance of calcium nodules was quantified by alizarin red S staining. Protein expression of glutathione peroxidase 4 (GPX4), long-chain fatty acyl-CoA synthetase 4 (ACSL4), and nicotinamide adenine dinucleotide phosphate oxidase 4 (NOX4) was analyzed by immunoblotting. Additionally, cells overexpressing NOX4 were evaluated for ferroptosis-related indicators (GPX4 and ACSL4 protein expression, GSH levels, MDA content) and osteogenic function (ALP activity and calcium nodule absorbance). Results H2O2 induced ferroptosis in MC3T3-E1 cells. Compared to the H2O2 group, treatment with Gusong Decoction-containing serum and Fer-1 significantly increased cell survival, SOD and CAT activities, GSH levels, and GPX4 protein expression (P<0.05), while decreasing cellular MDA content, Fe2+ and ROS levels, as well as NOX4 and ACSL4 protein expression (P<0.05). Overexpression of NOX4 attenuated the protective effects of Gusong Decoction-containing serum on ferroptosis and osteogenic function in H2O2 treated MC3T3-E1 cells. Conclusion Gusong Decoction-containing serum inhibits H2O2 induced ferroptosis in MC3T3-E1 cells, potentially through the suppression of the NOX4/ROS signaling pathway.
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